The Role of Antioxidants in Elastomers and Their Formulation Strategies

The Role of Antioxidants in Elastomers and Their Formulation Strategies


I. Functional Mechanisms of Antioxidants in Elastomer Systems

Antioxidants in raw materials: Primary antioxidants are typically incorporated during elastomer synthesis to provide oxidative protection during storage and transportation. These additives effectively retard/prevent material degradation caused by oxidation, thereby maintaining raw material stability and quality parameters.

Antioxidants in modified formulations: Their inclusion serves dual purposes during both processing and service life: Processing phase: During high-temperature manufacturing processes (pelletization, extrusion, injection molding), mechanical shear and thermal energy induce free radical formation. Antioxidants function as radical scavengers to inhibit oxidative chain reactions.

Service conditions: When exposed to environmental stressors (UV radiation, thermal cycling, humidity), formulated antioxidants provide supplementary protection against aging phenomena. Performance requirements vary significantly across applications - specialized antioxidants may be required for enhanced heat resistance (≥120°C continuous service) or weatherability.

II. Antioxidant Selection Criteria

Material compatibility: Selection must consider substrate characteristics. For instance, SBS-based TPR materials with unsaturated double bonds demand higher-performance antioxidants compared to conventional TPE systems.

Processing parameters: Thermal stability and shear resistance are critical considerations. Selected antioxidants must maintain efficacy under specific processing conditions (typical temperature range: 180-220°C).

Regulatory compliance: Contemporary formulations must adhere to global environmental regulations (REACH, RoHS) and toxicity standards (FDA, USP Class VI). Phosphite-free alternatives are increasingly preferred in eco-sensitive applications.

 

III. Technical Guidelines for Antioxidant Implementation

Commercial antioxidant systems: • Primary/Secondary synergists: Standard combination of 1010 (phenolic) + 168 (phosphite) at 1:1-2 ratio.

1010: High-performance bis-phenol antioxidant (mp: 110-125°C)

168: Hydroperoxide decomposer (enhances 1010 regeneration) • Alternative option: 1076 mono-phenol antioxidant (mp: 50-55°C) for cost-sensitive applications with moderate performance requirements

Dosage optimization: Typical loading ranges from 0.5-3 wt%, adjustable based on: • Base polymer characteristics • Processing parameters • End-use performance specifications

Processing considerations: • Temperature control: Maintain below antioxidant decomposition thresholds • Shear management: Ensure homogeneous dispersion without molecular degradation • Compatibility testing: Verify antioxidant-polymer interactions during compounding

This formulation approach ensures optimal balance between oxidative protection and mechanical